HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Benzyloxy)-5-methoxy-2-nitrobenzonitrile → HCID 22349623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Benzyloxy)-5-methoxy-2-nitrobenzonitrile | HCID 11673618 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 22349623 | HCID 22349623 | 62% |
Reaction Steps
2-nitro-4-benzyloxy-5-methoxybenzonitrile (3 g, 10.6 mmol) was treated with trifluoroacetic acid (30 ml) at reflux for 0.5 hour. The solvent was evaporated, the residue triturated with ether to give a yellow solid of title compound (1.27 g, 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919338B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-5faa2a5845174eb78fa8dbce174e4cf7 |
| Source note | uspto-grants-2005_07 |