HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 22349636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 86589729 | HCID 86589729 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22349636 | HCID 22349636 | 82.6% |
Reaction Steps
Methyl(2-tert-butoxycarbonylamino-1,3-thiazole-5-yl)(oxo)acetate (1.14 g, 4 mmol) in ethanol (10 ml) was treated with sodium hydroxyde (2N, 4 ml, 8 mmol) for 3M minutes at room temperature. Ethanol was removed, the aqueous solution was acidified (pH 3). The solid was recovered, dried to give title product (900 mg, 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919338B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-84db59fea1e7438b8bf3b8cdca3f5b70 |
| Source note | uspto-grants-2005_07 |