HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → Methyl 2-(4-(methylsulfonyl)phenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 4-Mesylphenylacetic acid | HCID 572345 | — |
| Product | Methyl 2-(4-(methylsulfonyl)phenyl)acetate | HCID 16640928 | — |
Reaction Steps
(4-Methanesulfonyl-phenyl)-acetic acid was treated with an etheral solution of diazomethane until completion of esterification by TLC. The solvent was evaporated, the residue triturated in hexane/ether and filtered to afford the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919353B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-cf9a18ad0e5c4b3daefe5bcd84d0025d |
| Source note | uspto-grants-2005_07 |