HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → Methyl 2-(4-(methylthio)phenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 4-(Methylthio)phenylacetic acid | HCID 4983912 | — |
| Product | Methyl 2-(4-(methylthio)phenyl)acetate | HCID 12067662 | — |
Reaction Steps
(4-Methylsulfanyl-phenyl)-acetic acid was treated with an etheral solution of diazomethane until completion of esterification. The solvent was evaporated, the residue triturated in hexane/ether, and filtered to afford the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919353B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-7d7dfc862ffb4d99af292e0bc0a387fb |
| Source note | uspto-grants-2005_07 |