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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 896664Generated: October 31, 2026

Water → HCID 22350093, compound

https://huagongshe.com/reaction/896664

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantEthanethiolHCID 6343—
ReactantCesium carbonateHCID 10796—
Reactant1-(Chloromethyl)-4-methanesulfonylbenzeneHCID 123530—
SolventDimethylformamideHCID 6228—
ProductHCID 22350093HCID 22350093—

Reaction Steps

To a solution of ethanethiol (0.3 mL, 4.9 mmol) and 4-methanesulfonylbenzyl chloride (1 g, 4,9 mmol) in DMF (10 mL) at 21° C. was added cesium carbonate (0.8 g, 2.5 mmol). After 18 h, the reaction mixture was poured into water and then filtered off to provide the 1-ethylsulfanylmethyl-4-methanesulfonyl-benzene compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06919353B2
Source datasetuspto-grants-2005_07
ORD IDord-c814f3c3e21247f085a1cc6bff83a5d6
Source noteuspto-grants-2005_07