HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22350093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 1-(Chloromethyl)-4-methanesulfonylbenzene | HCID 123530 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22350093 | HCID 22350093 | — |
Reaction Steps
To a solution of ethanethiol (0.3 mL, 4.9 mmol) and 4-methanesulfonylbenzyl chloride (1 g, 4,9 mmol) in DMF (10 mL) at 21° C. was added cesium carbonate (0.8 g, 2.5 mmol). After 18 h, the reaction mixture was poured into water and then filtered off to provide the 1-ethylsulfanylmethyl-4-methanesulfonyl-benzene compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919353B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-c814f3c3e21247f085a1cc6bff83a5d6 |
| Source note | uspto-grants-2005_07 |