Triethoxysilane → HCID 22345873, compound

Participants

Reaction Steps

Into the 100 ml of dried tetrahydrofuran, were fed 25.8 g (20 mmol) of t-butyl acrylate and 32.8 g (20 mmol) of triethoxysilane, and the mixture was substituted by argon. To the mixture solution, 10 mg of chloroplatinic acid was added and the mixture was heated for 24 hours under reflux. After completion of the reaction, 58.5 g of the objective compound was obtained by removing solvent.

Provenance & Evidence