HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22347442, compound → HCID 9907963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22347442 | HCID 22347442 | — |
| Reactant | HCID 22347460 | HCID 22347460 | — |
| Product | HCID 9907963 | HCID 9907963 | 16% |
Reaction Steps
From 400 mg (1.40 mmol) of 3-t-butoxycarbonylamino-4-methoxybenzenesulfonamide and 533 mg (1.40 mmol) of 4-chloro-2-N-phenoxycarbonylanthranilic acid benzylester in a similar manner to Preparation Example 17, 86 mg (yield 16%: 4 steps) of the title compound was obtained. Property: colorless crystals, melting point: >200° C. (decomposition), PMR (δppm, DMSO-d6): 3.81 (3H, s), 7.26-7.37 (5H, m), 7.77 (1H, s), 7.90 (1H, d), 7.94 (1H, d), 11.73 (1H, s)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06921766B1 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-b862a6317f704ab0b8e4f2538a66ca89 |
| Source note | uspto-grants-2005_07 |