HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethylbenzaldehyde → HCID 10000345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethylbenzaldehyde | HCID 22278 | — |
| Reactant | HCID 22348214 | HCID 22348214 | — |
| Product | HCID 10000345 | HCID 10000345 | — |
Reaction Steps
4-(Piperidin-4-ylamino)-6-vinyl-chromen-2-one and 3,4-dimethylbenzaldehyde were allowed to react in a manner analogous to that previously described to give the title compound. 1H NMR (500 MHz, DMSO-D6) δ ppm 1.65 (m, 2H) 1.92 (m, 2H) 2.08 (m, 2H) 2.20 (m, 6H) 2.84 (m, 2H) 3.42 (m, 2H) 3.50 (m, 1H) 5.23 (s, 1H) 5.34 (m, 1H) 5.94 (m, 1H) 6.76 (m, 1H) 7.01 (m, 1H) 7.07 (m, 2H) 7.24 (m, 2H) 7.69 (m, 1H) 8.20 (m, 1H); MS (DCI/NH3) m/z 389 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06921821B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-457eade4d6014615ab3eae65bdb4362b |
| Source note | uspto-grants-2005_07 |