HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86067347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 69293318 | HCID 69293318 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86067347 | HCID 86067347 | — |
Reaction Steps
4-Diethoxymethyl-2-hexylsulfanyl-pyrimidine (250 mg, 0.8 mmol) was stirred in THF (5 mL) and 4 N HCl (5 mL) at 20° C. for 64 h. The reaction mixture was poured in cold 10% Na2CO3 and extracted twice with AcOEt and once with sat. NaCl solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351700B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-040c2d2dd29a436f887b94dba45c3033 |
| Source note | uspto-grants-2008_04 |