Hydrochloric Acid → HCID 22675683, compound

HRID 898409Notes

Reaction equation

HRID 898409 reaction equation
[CH:1]([C:5]1[CH:10]=[CH:9][C:8]([NH:11][CH2:12][C:13]2[CH:18]=[CH:17][C:16]([C:19]([CH3:22])([CH3:21])[CH3:20])=[CH:15][CH:14]=2)=[CH:7][CH:6]=1)([CH2:3][CH3:4])[CH3:2].[ClH:23]>C(OCC)C>[CH:1]([C:5]1[CH:10]=[CH:9][C:8]([NH:11][CH2:12][C:13]2[CH:14]=[CH:15][C:16]([C:19]([CH3:21])([CH3:20])[CH3:22])=[CH:17][CH:18]=2)=[CH:7][CH:6]=1)([CH2:3][CH3:4])[CH3:2].[ClH:23]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 10547519HCID 10547519, compound

Product 1

HCID 22675683HCID 22675683, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Conditions

Temperature
25 °C

Procedure

To a solution of N-(4-sec-butylphenyl)-4-tert-butylbenzylamine (4.5 g) in diethylether (10 mL) was added ether at HCl solution at 4° C., then the reaction mixture was stirred at 25° C. for 10 minutes. The resulting solution was the evaporated and dried under vacuum to afford 4.7 g of N-(4-sec-butylphenyl)-4-tert-butylbenzylamine·HCl.

Workup

  1. customevaporated
  2. customdried under vacuum

Sources & evidence

ORD record
ord-42deaf03a75244919e82a1f151c92b60
Source dataset
uspto-grants-2008_04
Patent number
US07351743B1

Reaction notes

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