HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → 5-Aminoacenaphthene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Acenaphthene, 3-nitro- | HCID 97618 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 5-Aminoacenaphthene | HCID 62547 | — |
Reaction Steps
A mixture of 5 and 3-nitroacenaphthene was reduced with Pd/C in ethyl acetate under hydrogen at 40 psi pressure and the resulting amines were separated by recrystallization from cyclohexane/ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351743B1 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-740902d564ae4dc9875a50fb861a96b0 |
| Source note | uspto-grants-2008_04 |