HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → Ethyl 3-hydroxypentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | Ethyl 3-oxovalerate | HCID 78656 | — |
| Product | Ethyl 3-hydroxypentanoate | HCID 316884 | 50% |
Reaction Steps
Ethyl 3-hydroxyvalerate was prepared following the procedure as described in step 1) of Preparation Example 2, except for that ethyl propionylacetate was used to replace for ethyl acetoacetate. Yield 50%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351778B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-0858150be08f46adb9c69611360987a0 |
| Source note | uspto-grants-2008_04 |