HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → Ethyl 3-hydroxyhexanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | Ethyl 3-oxohexanoate | HCID 238498 | — |
| Product | Ethyl 3-hydroxyhexanoate | HCID 61293 | 48% |
Reaction Steps
Ethyl 3-hydroxycaproate was prepared following the procedure as described in step 1) of Preparation Example 2, except for that ethyl butyrylacetate was used to replace for ethyl acetoacetate. Yield 48%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351778B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-c037db2a595140a98eb3440a2b2b627e |
| Source note | uspto-grants-2008_04 |