HCID 2829603, compound → HCID 16090593, compound

Participants

Reaction Steps

1.20 mg (4.416 mmol) of N′-(2-chloro-4-nitro-phenyl)-N,N-diethyl-ethane-1,2-diamine was added to a suspension of 200 mg Raney-Ni in 20 mL MeOH and the mixture was hydrogenated for 2 hours at RT under 20 psi H2 atmosphere. The catalyst was filtered off and the filtrate evaporated down i. vac.

Provenance & Evidence