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HRID898554

反应详情

EQUATION

反应方程式

HRID 898554 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)/C=C/c1ccc(C(F)(F)F)cc1Cl
HCID5709520

未命名化合物

结构：O=[N+]([O-])c1ccc(CCCO)c(Cl)c1
HCID68877970

未命名化合物

PRODUCTS

生成物

1
结构：O=C(/C=C/c1ccc(C(F)(F)F)cc1Cl)Nc1ccc(CCCO)c(Cl)c1
HCID68878212

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Intermediate product Z32a starting from (E)-3-(2-chloro-4-trifluoromethyl-phenyl)-acrylic acid (Z37b) and 3-(2-chloro-4-nitro-phenyl)-propan-1-ol. The crude product was purified by column chromatography (silica gel, petroleum ether/EtOAc 1:1).

WORKUP

后处理

  1. customPrepared analogously to Intermediate product Z32a
  2. customThe crude product was purified by column chromatography (silica gel, petroleum ether/EtOAc 1:1)