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HRID898620

反应详情

EQUATION

反应方程式

HRID 898620 的结构方程式

REACTANTS

反应物

2
结构：CN1CCN(Cc2ccc(N)cc2)CC1
HCID3153996

4-(4-Methylpiperazin-1-ylmethyl)phenylamine

C12H19N3

结构：O=C(O)/C=C/c1ccc(-c2ccc(Cl)cc2)cc1
HCID5957595

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCN(Cc2ccc(NC(=O)/C=C/c3ccc(-c4ccc(Cl)cc4)cc3)cc2)CC1
HCID59691672

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 172 starting from (E)-3-(4′-chloro-biphenyl-4-yl)-acrylic acid and 4-(4-methyl-piperazin-1-ylmethyl)-phenylamine. The crude product was purified by column chromatography (silica gel, dichloromethane/MeOH/conc. aqueous ammonia 90:10:0.1).

WORKUP

后处理

  1. customThe crude product was purified by column chromatography (silica gel, dichloromethane/MeOH/conc. aqueous ammonia 90:10:0.1)