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HRID898624

反应详情

EQUATION

反应方程式

HRID 898624 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)/C=C/c1ccccn1
HCID5356626

未命名化合物

结构：CCN(CC)CCOc1ccc(N)cc1Cl
HCID16791676

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)CCOc1ccc(NC(=O)/C=C/c2ccccn2)cc1Cl
HCID59691598

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 172 starting from (E)-3-pyridin-2-yl-acrylic acid and 3-chloro-4-(2-diethylamino-ethoxy)-phenylamine (Z2b) at RT (72 h). The crude product was purified by column chromatography (silica gel, dichloromethane/MeOH/conc. aqueous ammonia 90:10:0.1) and recrystallisation from petroleum ether.

WORKUP

后处理

  1. customThe crude product was purified by column chromatography (silica gel, dichloromethane/MeOH/conc. aqueous ammonia 90:10:0.1) and recrystallisation from petroleum ether