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HRID898626

反应详情

EQUATION

反应方程式

HRID 898626 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCc1ccc(N)cc1
HCID14939861

4-(2-Dimethylaminoethyl)aniline

C10H16N2

结构：O=C(O)/C=C/c1ccc(-c2ccc(Cl)cc2)cn1
HCID59691634

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCc1ccc(NC(=O)/C=C/c2ccc(-c3ccc(Cl)cc3)cn2)cc1
HCID59691592

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 143 starting from (E)-3-[5-(4-chloro-phenyl)-pyridin-2-yl]-acrylic acid (Z34b) and 4-(2-dimethylamino-ethyl)-phenylamine. The crude product was purified by column chromatography (silica gel, dichloromethane/EtOH/conc. aqueous ammonia 50:10:0.1).

WORKUP

后处理

  1. customThe crude product was purified by column chromatography (silica gel, dichloromethane/EtOH/conc. aqueous ammonia 50:10:0.1)