HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 5709520, compound → (e)-n-(3-Chloro-4-diethylaminomethyl-phenyl)-3-(2-chloro-4-trifluoromethyl-phenyl)-acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 5709520 | HCID 5709520 | — |
| Reactant | 3-Chloro-4-diethylaminomethyl-phenylamine | HCID 28721821 | — |
| Product | (e)-n-(3-Chloro-4-diethylaminomethyl-phenyl)-3-(2-chloro-4-trifluoromethyl-phenyl)-acrylamide | HCID 59691581 | — |
Reaction Steps
Prepared analogously to Example 143 starting from (E)-3-(2-chloro-4-trifluoromethyl-phenyl)-acrylic acid (Z37b) and 3-chloro-4-diethylaminomethyl-phenylamine (Z35b). The crude product was purified by column chromatography (Alox, neutral, act. II-III, petroleum ether/EtOAc 3:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351719B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-e12f58a1fc7443fcbe33adafa995091f |
| Source note | uspto-grants-2008_04 |