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HRID898629

反应详情

EQUATION

反应方程式

HRID 898629 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)/C=C/c1ccc(C(F)(F)F)cc1Cl
HCID5709520

未命名化合物

结构：CC1CCN(Cc2ccc(N)cc2Cl)CC1
HCID28721844

未命名化合物

PRODUCTS

生成物

1
结构：CC1CCN(Cc2ccc(NC(=O)/C=C/c3ccc(C(F)(F)F)cc3Cl)cc2Cl)CC1
HCID59691545

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 143 starting from (E)-3-(2-chloro-4-trifluoromethyl-phenyl)-acrylic acid (Z37b) and 3-chloro-4-(4-methyl-piperidin-1-ylmethyl)-phenylamine (Z36b). The crude product was purified by column chromatography (Alox, neutral, act. II-III, petroleum ether/EtOAc 3:1).

WORKUP

后处理

  1. customThe crude product was purified by column chromatography (Alox, neutral, act. II-III, petroleum ether/EtOAc 3:1)