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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 898666Generated: October 30, 2026

HCID 69215509, compound → HCID 69215235, compound

https://huagongshe.com/reaction/898666

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69215509HCID 69215509—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 69215235HCID 69215235—

Reaction Steps

Following General Procedure G and using acetoxymethyl-4-benzyloxy-2-fluoro-phenyl acetate (Compound 20, 0.75 g, 2.26 mmol), ethyl acetate (15 mL) and 10% palladium on carbon (0.08 g), the title compound was obtained as an oil (0.48 g, 88%). 1H-NMR (300 MHz, CDCl3): δ2.09 (s, 3H), 3.62 (s, 2H), 5.75 (s, 2H), 6.48-6.54 (m, 2H), 7.02 (d, J=8.4 Hz, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07351737B2
Source datasetuspto-grants-2008_04
ORD IDord-6c05b8806f494ffd8869646ea05219dd
Source noteuspto-grants-2008_04