HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69215509, compound → HCID 69215235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69215509 | HCID 69215509 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69215235 | HCID 69215235 | — |
Reaction Steps
Following General Procedure G and using acetoxymethyl-4-benzyloxy-2-fluoro-phenyl acetate (Compound 20, 0.75 g, 2.26 mmol), ethyl acetate (15 mL) and 10% palladium on carbon (0.08 g), the title compound was obtained as an oil (0.48 g, 88%). 1H-NMR (300 MHz, CDCl3): δ2.09 (s, 3H), 3.62 (s, 2H), 5.75 (s, 2H), 6.48-6.54 (m, 2H), 7.02 (d, J=8.4 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351737B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-6c05b8806f494ffd8869646ea05219dd |
| Source note | uspto-grants-2008_04 |