HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86607501, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86623929 | HCID 86623929 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86607501 | HCID 86607501 | 100% |
Reaction Steps
[(1R*,2R*,3R*)-2-methoxymethyl-1-(methoxy-methyl-carbamoyl)-3-phenyl-cyclopropyl]-carbamic acid t-butyl ester (25 mg, 0.69 mmol) was dissolved in 4 mL of HCl in dioxane (4M). After stirring at room temperature for 1 hour, the solution was concentrated and dried under high vacuum to afford 100% of an HCl salt product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07351825B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-c38b12e34a4b4203988932b54dcced04 |
| Source note | uspto-grants-2008_04 |