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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 899144Generated: October 29, 2026

Benzylethanolamine → HCID 69070027, compound

https://huagongshe.com/reaction/899144

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzylethanolamineHCID 4348—
ReactantN,N'-DimethylureaHCID 7293—
ProductHCID 69070027HCID 69070027—

Reaction Conditions

Temperature130 °C

Reaction Steps

A mixture of N-benzyl ethanolamine (3 g, 0.0198 mol) and N,N′-dimethyl urea was stirred at 130° C. overnight. The reaction mixture was cooled to RT and the crude product was purified by column chromatography over silica gel using 3% methanol in dichloromethane as eluent to yield 3.5 g of the sub-title compound as a liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07354917B2
Source datasetuspto-grants-2008_04
ORD IDord-47be5271e39f41f0b1af2557fb0d6744
Source noteuspto-grants-2008_04