HRID899256
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of tert-butyl 3-methoxyazetidine-1-carboxylate (step 1, 110 mg, 0.57 mmol) in dichloromethane (6.0 mL) was added trifluoroacetic acid (6.0 mL). The resulting solution was stirred at room temperature for 4 h. The volatile materials were removed under the reduced pressure to afford 120 mg (quant.) of the title compound as a highly viscous oil:
WORKUP
后处理
- customThe volatile materials were removed under the reduced pressure