HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69216306, compound → HCID 69214221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69216306 | HCID 69216306 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69214221 | HCID 69214221 | 97.5% |
Reaction Steps
A solution of 2-(3-nitro-phenyl)-heptanoic acid ethyl ester (4.451 g, 15.9 mmole) in 150 mL of ethyl acetate containing 1.69 g of 10% palladium on carbon was subjected to atmospheric pressure of hydrogen for 15 hours. The mixture was filtered through a Celite/SiO2 pad and the volatiles were removed in vacuo to yield 3.866 g of 2-(3-amino-phenyl)-heptanoic acid ethyl ester as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07354931B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-028349c1834441509f651ccd7659d161 |
| Source note | uspto-grants-2008_04 |