HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 899607Generated: October 28, 2026
Acetic Anhydride → HCID 10081676, compound
https://huagongshe.com/reaction/899607
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 1-Oxo-6,7,8,9-tetrahydro-5H-1lambda~5~-cyclohepta[b]pyridine | HCID 589689 | — |
| Product | HCID 10081676 | HCID 10081676 | — |
Reaction Steps
The N-oxide was dissolved in acetic anhydride (222 mL) and heated at 90° C. overnight. The mixture was cooled to room temperature and concentrated. Distillation (Kugelrohr, bp 110-140° C.@1 Torr) of the resultant oil provided 53.26 g of acetic acid 6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridin-9-yl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07354932B2 |
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| Source dataset | uspto-grants-2008_04 |
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| ORD ID | ord-2f267a8c76b545b8bf7fee25cb9767d6 |
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| Source note | uspto-grants-2008_04 |
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