Hydroxylamine → HCID 178513281, compound

Participants

Reaction Steps

Benzonitrile (5 g, 48 mmol) was dissolved in ethanol (100 ml) and treated with 50% aqueous hydroxylamine (16 ml, 242 mmol). Reaction was heated to reflux for 3 hours before concentration under reduced pressure to give a clear foam (4.5 g, 68%).

Provenance & Evidence