HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulpiride → HCID 11451902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulpiride | HCID 5355 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 11451902 | HCID 11451902 | — |
Reaction Steps
A solution of N-(1-Ethyl-pyrrolidin-2-ylmethyl)-2-methoxy-5-sulfamoyl-benzamide, acetic anhydride and triethylamine are reacted at room temperature, diluted with water and extracted with ethyl acetate. The ethyl acetate layer is dried, filtered and concentrated under vacuum, and the residue recrystallized from ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358271B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-67e3a46fbe574971a68f827107853483 |
| Source note | uspto-grants-2008_04 |