HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethylbenzoyl chloride → HCID 22182230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethylbenzoyl chloride | HCID 97038 | — |
| Reactant | HCID 11030629 | HCID 11030629 | — |
| Product | HCID 22182230 | HCID 22182230 | 92% |
Reaction Steps
Using this hydroxylamine compound and 2,4,6-trimethylbenzoyl chloride in a procedure otherwise similar to that for preparing the compound 101 gives a 92% yield of the compound 104 which is obtained in the form of colourless crystals; melting point: 181-183° C. (dichloromethane/methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358365B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-99b6ab1f611541ce9e63fe0507de084d |
| Source note | uspto-grants-2008_04 |