HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 22182242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 1-Hydroxy-4-benzoyloxy-2,2,6,6-tetramethylpiperidine | HCID 688178 | — |
| Product | HCID 22182242 | HCID 22182242 | 70% |
Reaction Steps
Using 1-hydroxy-4-benzoyloxy-2,2,6,6-tetramethylpiperidine (prepared as described by: Kurumada T. et. al., loc. cit.) and pivaloyl chloride in a procedure otherwise similar to the preparation of the compound 101 gives a 70% yield of the compound 107 which is obtained in the form of colourless crystals; melting point: 107-110° C. (hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358365B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-6d69f4a5b4b14c29913e088faf6df93f |
| Source note | uspto-grants-2008_04 |