HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → 3-(Carbamoylamino)-5-Phenylthiophene-2-Carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Trimethylsilyl isocyanate | HCID 70696 | — |
| Reactant | 3-Amino-5-phenylthiophene-2-carboxamide | HCID 2756534 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-(Carbamoylamino)-5-Phenylthiophene-2-Carboxamide | HCID 10220851 | — |
Reaction Steps
3-Amino-5-phenyl-2-thiophenecarboxamide (0.5 g), trimethylsilylisocyanate (3 mL), dichloromethane (15 mL) and dimethylformamide (3 mL) were heated at reflux for 3 days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07358376B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-8901e10bc1ad4465acd6210ec4f1a2eb |
| Source note | uspto-grants-2008_04 |