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HRID900414

反应详情

EQUATION

反应方程式

HRID 900414 的结构方程式

REACTANTS

反应物

3
结构：ClCCl
HCID6344

Dichloromethane

CH2Cl2

结构：C[Si](C)(C)N=C=O
HCID70696

Trimethylsilyl isocyanate

C4H9NOSi

结构：NC(=O)c1sc(-c2ccccc2)cc1N
HCID2756534

3-amino-5-phenylthiophene-2-carboxamide

C11H10N2OS

PRODUCTS

生成物

1
结构：NC(=O)Nc1cc(-c2ccccc2)sc1C(N)=O
HCID10220851

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

3-Amino-5-phenyl-2-thiophenecarboxamide (0.5 g), trimethylsilylisocyanate (3 mL), dichloromethane (15 mL) and dimethylformamide (3 mL) were heated at reflux for 3 days.

WORKUP

后处理

  1. temperatureat reflux for 3 days