Ethanol → N,N'-Dimethoxy-N,N'-dimethyloxamide

HRID 900509Notes

Reaction equation

[CH2:1]([OH:3])C.C[N:5]([CH3:8])[CH:6]=[O:7]>>[CH3:1][O:3][N:5]([CH3:8])[C:6]([C:6]([N:5]([O:3][CH3:1])[CH3:8])=[O:7])=[O:7]

Participants

Reactant 2

HCID 702Ethanol

HCID 6228Dimethylformamide

Product 1

HCID 3287678N,N'-Dimethoxy-N,N'-dimethyloxamideYield 77.5%

Procedure

The reaction was carried out in the same manner as in Example 3 except for changing ethanol to dimethylformamide in Example 3. As a result, 1.16 g (Reaction yield: 77.5%) of N,N′-dimethoxy-N,N′-dimethyl oxamide was found to be formed.

Sources & evidence

ORD record: ord-a7273332ab1b49f88a34ff901c81eb6f
Source dataset: uspto-grants-2008_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07358394B2

Reaction notes

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