Ethyl chloroformate → HCID 72985482, compound

Participants

Reaction Steps

The operation was conducted in the same manner as in Example 8 except that the amount of ethyl chlorocarbonate was 1.3-fold mol relative to the starting material. As a result, the conversion ratio of 3-(diethoxymethyl)-2-ethoxytetrahydrofuran was 97.1%, and 4-chloro-2-ethoxymethylidenebutanal was obtained in a yield of 90.5%.

Provenance & Evidence