Sodium Carbonate → HCID 58608977, compound

HRID 900636Notes

Reaction equation

HRID 900636 reaction equation
Cl.Cl.[NH2:3][C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)=[C:6]([NH2:20])[CH:5]=1.C(=O)([O-])[O-].[Na+].[Na+]>O>[NH2:3][C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)=[C:6]([NH2:20])[CH:5]=1

Participants

4

Reactant 2

HCID 10340Sodium CarbonateHCID 68566317HCID 68566317, compound

Product 1

HCID 58608977HCID 58608977, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To 1 g of 1,3-diamino-4-[2-(4-methoxyphenyl)ethyl]benzene dihydrochloride from Example 3 in 50 mL of water was added saturated sodium carbonate solution to pH 8. The mixture was suction-filtered and the filter cake was washed with a small amount of cold water and then dried under vacuum over phosphorus pentoxide.

Workup

  1. filtrationThe mixture was suction-filtered
  2. washthe filter cake was washed with a small amount of cold water
  3. dry with materialdried under vacuum over phosphorus pentoxide

Sources & evidence

ORD record
ord-b8afcc2439ef4d86b080bcfc171e27a5
Source dataset
uspto-grants-2008_04
Patent number
US07361198B2

Reaction notes

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