Sodium Carbonate → HCID 58608977, compound

Participants

Reaction Steps

To 1 g of 1,3-diamino-4-[2-(4-methoxyphenyl)ethyl]benzene dihydrochloride from Example 3 in 50 mL of water was added saturated sodium carbonate solution to pH 8. The mixture was suction-filtered and the filter cake was washed with a small amount of cold water and then dried under vacuum over phosphorus pentoxide.

Provenance & Evidence