Azobisisobutyronitrile → HCID 86596289, compound

Participants

Reaction Steps

To 50 g of propylene glycol methyl ether acetate (PGMEA) were added 5 g of 9-anthracenemethyl methacrylate, 1 g of 2-hydroxyethyl methacrylate, 3 g of t-butylacrylate, 1 g of acrylic acid and 0.4 g of AIBN. The prepared solution was reacted at 66° C. for 8 hours. After the reaction, the resulting mixture was precipitated in ethyl ether, filtered, and dried under vacuum condition, thereby obtaining poly(9-anthracenemethyl methacrylate/2-hydroxyethyl methacrylate/t-butylacrylate/acrylic acid) having a molecular weight of 12,500 (yield: 88%) (see the NMR spectrum of FIG. 1).

Provenance & Evidence