Azobisisobutyronitrile → HCID 86596290, compound

Participants

Reaction Steps

To 50 g of PGMEA were added 6 g of 9-anthracenemethyl methacrylate, 3 g of t-butylacrylate, 1 g of acrylic acid and 0.8 g of AIBN. The prepared solution was reacted at 66° C. for 8 hours. After the reaction, the resulting mixture was precipitated in ethyl ether, filtered, and dried under vacuum condition thereby obtaining poly(9-anthracenemethyl methacrylate/t-butylacrylate/acrylic acid) having a molecular weight of 11,200 (yield: 80%) (see the NMR spectrum of FIG. 2).

Provenance & Evidence