HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178527843 | HCID 178527843 | — |
| Product | HCID 178503395 | HCID 178503395 | — |
Reaction Steps
To a dichloromethane solution of 5-pyridin-3-yl-2H-[1,2,4]triazole-3-thiol (Step B, Example 1) triethylamine was added followed by iodomethane. This solution was stirred at room temperature for 2 h, during which period the reaction was complete by RP-HPLC. The solvent was evaporated and the residue was purified by RP-HPLC affording the desired intermediate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07361669B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-4384b5969b6a42de81f324561fde1ab6 |
| Source note | uspto-grants-2008_04 |