HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-methyl-2,3-dihydro-1H-1,3-benzodiazol-2-one → Methyl 6-[2,3-dihydro-3-methyl-2-oxo-1H-benzimidazol-1-ylmethyl]-1,2,3,4-tetrahydro-3-methyl-1-(2-methylpropyl)-2,4-dioxo-thieno[2,3-d]pyrimidine-5-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-methyl-2,3-dihydro-1H-1,3-benzodiazol-2-one | HCID 590540 | — |
| Reactant | Methyl 6-bromomethyl-1-isobutyl-3-methyl-2,4-dioxo-1,2,3,4-tetrahydrothieno[2,3-d]pyrimidine-5-carboxylate | HCID 16102871 | — |
| Product | Methyl 6-[2,3-dihydro-3-methyl-2-oxo-1H-benzimidazol-1-ylmethyl]-1,2,3,4-tetrahydro-3-methyl-1-(2-methylpropyl)-2,4-dioxo-thieno[2,3-d]pyrimidine-5-carboxylate | HCID 69197857 | — |
Reaction Steps
The subtitle compound was prepared by the method of example 1 step c) using the product of example 1 step b) and N-methylbenzimidazolone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07361660B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-bf275b09665e415c97a09eebe07ae8d6 |
| Source note | uspto-grants-2008_04 |