HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 178503194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | 4-(Methylthio)benzonitrile | HCID 590960 | — |
| Product | HCID 178503194 | HCID 178503194 | 83.26% |
Reaction Steps
The title compound was prepared from 4-methylthiobenzonitrile (11.7 g, 78 mmol) and 4-chloroaniline (10 g, 78 mmol) by following the procedure described in preparation 10 (18.06 g, yield 83.26%, purity 98.9% by HPLC). MS m/z:277.1/278.7 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365069B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-e1ded83f32124277a7c0110535361d0d |
| Source note | uspto-grants-2008_04 |