4-Cyanopyridine → HCID 178512045, compound
Reaction equation
[C:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)#[N:2].[F:9][C:10]1[CH:16]=[CH:15][C:13]([NH2:14])=[CH:12][CH:11]=1>>[F:9][C:10]1[CH:16]=[CH:15][C:13]([NH:14][C:1]([C:3]2[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=2)=[NH:2])=[CH:12][CH:11]=1Participants
3
Procedure
The title compound was prepared from 4-cyanopyridine (0.94 g, 9 mmol) and 4-fluoroaniline (1 g, 9 mmol) by following the procedure described in preparation 10 (1.1 g, yield 56.5%).
Sources & evidence
- ORD record
- ord-531a4dbabf5d4bbaac78d3e6332b9a08
- Source dataset
- uspto-grants-2008_04
- Patent number
- US07365069B2
Reaction notes
Loading…