HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 66563827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 69313202 | HCID 69313202 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66563827 | HCID 66563827 | 78.2% |
Reaction Steps
The reaction was carried out in similar procedure to Example 75b using 237 mg (0.58 mmol) of benzyl 4-[(2-{[tert-butyl(dimethyl)silyl]oxy}ethoxy)methyl]piperidine-1-carboxylate obtained in Example 77a and 0.87 mL (0.87 mmol) of a solution of 1M tetrabutylammonium fluoride in tetrahydrofuran to obtain 133 mg (yield: 78%) of the title compound as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365067B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-52282a8da9544eaea4f9c381dea684a3 |
| Source note | uspto-grants-2008_04 |