HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11431603, compound → HCID 69316333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11431603 | HCID 11431603 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69316333 | HCID 69316333 | — |
Reaction Steps
To a suspension of [4-(2-bromo-4-isopropyl-phenyl)-6-methyl-1-(1-propyl-butyl)-1H-1,5,7b-triaza-cyclopenta[cd]inden-2-ylidene]-methyl-amine (135 mg) in a mixture of ethyl acetate (1.5 mL) and ethanol (0.2 mL) was added 4M HCl/ethyl acetate (0.25 mL) and concentrated under reduced pressure. The residue was solidified from Et2O to provide the title compound as an amorphous (73 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365078B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-5242085275ae4c6c8a16192906bf8391 |
| Source note | uspto-grants-2008_04 |