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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 902095Generated: October 30, 2026

HCID 11431603, compound → HCID 69316333, compound

https://huagongshe.com/reaction/902095

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 11431603HCID 11431603—
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
SolventEthanolHCID 702—
SolventEthyl AcetateHCID 8857—
ProductHCID 69316333HCID 69316333—

Reaction Steps

To a suspension of [4-(2-bromo-4-isopropyl-phenyl)-6-methyl-1-(1-propyl-butyl)-1H-1,5,7b-triaza-cyclopenta[cd]inden-2-ylidene]-methyl-amine (135 mg) in a mixture of ethyl acetate (1.5 mL) and ethanol (0.2 mL) was added 4M HCl/ethyl acetate (0.25 mL) and concentrated under reduced pressure. The residue was solidified from Et2O to provide the title compound as an amorphous (73 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07365078B2
Source datasetuspto-grants-2008_04
ORD IDord-5242085275ae4c6c8a16192906bf8391
Source noteuspto-grants-2008_04