HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanamide → HCID 178457581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanamide | HCID 9864 | — |
| Reactant | 1,1,1-Trimethoxypropane | HCID 141145 | — |
| Reactant | 1-(2,4-dichlorophenyl)ethanamine | HCID 2771858 | — |
| Product | HCID 178457581 | HCID 178457581 | 84.4% |
Reaction Steps
1.85 g of 1-(2,4-dichlorophenyl)ethylamine, 1.63 g of trimethyl orthopropionate and 0.46 g of Cyanamide were heated under reflux for about 30 minutes. The volatile components were removed under reduced pressure and the residue was then titrated with water. Filtration and drying gave 2.22 g of N′-cyano-N-[1-(2,4-dichlorophenyl)ethyl]propaneimidamide of logP of 2.56.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365098B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-4c1f3f52d390450c9858927829b700de |
| Source note | uspto-grants-2008_04 |