Ethyl Acetoacetate → HCID 22322934, compound

HRID 902224Notes

Reaction equation

[C:1]([O:7][CH2:8][CH3:9])(=[O:6])[CH2:2][C:3]([CH3:5])=[O:4].Br[CH2:11][CH:12]1[O:17][CH2:16][CH2:15]C[O:13]1>>[O:17]1[CH:16]=[CH:15][O:13][CH:12]1[CH2:11][CH2:5][C:3](=[O:4])[CH2:2][C:1]([O:7][CH2:8][CH3:9])=[O:6]

Participants

Reactant 2

HCID 8868Ethyl Acetoacetate

HCID 3036832-bromomethyl-1,3-dioxane

Product 1

HCID 22322934HCID 22322934, compound

Procedure

The title compound was synthesized from ethyl acetoacetate and 2-bromomethyl-1,3-dioxane, according to the procedure of Huckin and Weiler, Tetrahedron Lett. 3927, (1971).

Sources & evidence

ORD record: ord-84907aeadd71493aae5e2ce59c51eb92
Source dataset: uspto-grants-2008_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07365093B2

Reaction notes

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