HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11455961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| Reactant | 1-[1-(3-Chlorophenyl)-2-piperazin-1-ylethyl]cyclohexanol | HCID 10381502 | — |
| Product | HCID 11455961 | HCID 11455961 | — |
Reaction Steps
In an analogous manner to Example 117, 1-{1-(3-chlorophenyl)-2-[4-(3-phenoxnbenzyl)piperazin-1-yl]ethyl}cyclohexanol dihydrochloride was prepared from 1-[1-(3-chlorophenyl)-2-piperazin-1-ylethyl]cyclohexanol (see Example 1) and 3-phenoxybenzaldehyde. MS (ESI) m/z 505/507 ([M+H]+); HRMS: calcd for C31H37ClN2O2. 2.00 HCl, 576.2077; found (ESI_FT), 505.26266.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365076B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-4e76740137d040b6a988ade633a1a0a0 |
| Source note | uspto-grants-2008_04 |