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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 902353Generated: October 30, 2026

1-Bromo-2-chlorobenzene → HCID 68961891, compound

https://huagongshe.com/reaction/902353

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-2-chlorobenzeneHCID 12754—
Reactant2-Chloro-6-methoxyphenylboronic acidHCID 3378271—
SolventWater 1,2-dimethoxyethaneHCID 18180031—
ProductHCID 68961891HCID 6896189174%

Reaction Steps

Treatment of 2-bromochlorobenzene (15.5 g, 80.6 mmol) with 2-chloro-6-methoxybenzene boronic acid (5.0 g, 26.8 mmol) in DME-water (5:1, 250 mL) according to the procedure described for Example 69, Step 1 provided 5.0 g (74%) of 2.2′-dichloro-6-methoxybiphenyl as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07365095B2
Source datasetuspto-grants-2008_04
ORD IDord-40ec2fd9741944099c68a9c60f4aa146
Source noteuspto-grants-2008_04