HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68964218, compound → HCID 69117516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68964218 | HCID 68964218 | — |
| Catalyst | HCID 178424406 | HCID 178424406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69117516 | HCID 69117516 | 48.4% |
Reaction Steps
Treatment of 3-allyl-2′,6-dichloro-biphenyl-2-ol (6.2 g, 22.2 mmol) in methylene chloride (200 mL) with dichlorobis(acetonitrile)palladium (II) (0.86 g, 3.3 mmol) according to the procedure described for Example 69, Step 5 provided 3.0 g (48%) of 2′,6-dichloro-3-(prop-1-enyl)biphenyl-2-ol as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365095B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-eb55b092b8fc41a3a96a6a0283a925b6 |
| Source note | uspto-grants-2008_04 |