HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69117595, compound → HCID 69116903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69117595 | HCID 69117595 | — |
| Catalyst | HCID 178424406 | HCID 178424406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69116903 | HCID 69116903 | 39.4% |
Reaction Steps
Treatment of 3-allyl-2′-chloro-6-fluoro-biphenyl-2-ol (3.8 g, 14.5 mmol) in methylene chloride (150 mL) with dichlorobis(acetonitrile)palladium (II) (0.56 g, 2.2 mmol) according to the procedure described for Example 69, Step 5 provided 1.5 g (39%) of 2′-chloro-6-fluoro-3-(prop-1-enyl)biphenyl-2-ol as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365095B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-dabe08510cf24ab3ac2faa7c79fab566 |
| Source note | uspto-grants-2008_04 |